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In vitro validation of the X-ray induced self-association behavior of an indomethacin-containing solid dispersion.
In the present work, an in vitro solid dispersion approach was employed to study the relationship between aqueous solubility of an indomethacin-containing solid dispersion and its self-association behavior. Five drugs in two scales of amorphous solid dispersions (ASDs) and crystalline forms (CMs) were prepared via a simple and general method in which the drug was co-stirred with the polymer carrier in the presence of a solvent or solvent mixture. The solubility differences between the ASDs and CMs were evaluated by determining the dissolution rate of indomethacin. The in vitro self-association behavior of the ASDs was first validated by the microscopic observation of the samples using the visual microscopy and transmission electronic microscopy. The self-association behavior of the ASDs was then characterized by DSC, XRPD, NMR, and Raman spectroscopy. The results show that the self-association behavior of the ASDs greatly affected the solubility. The solid state XRPD and DSC results indicate that the self-association behavior of the samples correlates with the in vitro solubility. The microscopic and solid state NMR and Raman spectroscopy results indicated that the amorphous and crystalline environments of the self-association were closely related to the solid state properties of the samples.Q:

If $f$ is $g$-differentiable on $E$, is $g$-continuous on $E$?

Let $f:E\to \mathbb{

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